Information card for entry 7038481

Structure parameters

• Formula: C31.5 H50 Bi Cl2 N Si
• Calculated formula: C31.5 H50 Bi Cl2 N Si
• Title of publication: Synthesis of mono-, di-, and triaminobismuthanes and observation of C-C coupling of aromatic systems with bismuth(iii) chloride.
• Authors of publication: Hering-Junghans, Christian; Schulz, Axel; Thomas, Max; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6053 - 6059
• a: 10.177 ± 0.0005 Å
• b: 10.7624 ± 0.0005 Å
• c: 16.328 ± 0.0007 Å
• α: 93.75 ± 0.002°
• β: 101.264 ± 0.002°
• γ: 105.923 ± 0.002°
• Cell volume: 1673.17 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0258
• Residual factor for significantly intense reflections: 0.0209
• Weighted residual factors for significantly intense reflections: 0.047
• Weighted residual factors for all reflections included in the refinement: 0.0485
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No