Information card for entry 7038482

Structure parameters

• Formula: C42 H76 N2 Si2
• Calculated formula: C42 H76 N2 Si2
• Title of publication: Synthesis of mono-, di-, and triaminobismuthanes and observation of C-C coupling of aromatic systems with bismuth(iii) chloride.
• Authors of publication: Hering-Junghans, Christian; Schulz, Axel; Thomas, Max; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6053 - 6059
• a: 10.3047 ± 0.0009 Å
• b: 28.762 ± 0.003 Å
• c: 14.6355 ± 0.0011 Å
• α: 90°
• β: 94.693 ± 0.004°
• γ: 90°
• Cell volume: 4323.2 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1196
• Residual factor for significantly intense reflections: 0.0549
• Weighted residual factors for significantly intense reflections: 0.118
• Weighted residual factors for all reflections included in the refinement: 0.1466
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No