Information card for entry 7038483

Structure parameters

• Formula: C30 H52 Bi Cl N2 Si2
• Calculated formula: C30 H52 Bi Cl N2 Si2
• Title of publication: Synthesis of mono-, di-, and triaminobismuthanes and observation of C-C coupling of aromatic systems with bismuth(iii) chloride.
• Authors of publication: Hering-Junghans, Christian; Schulz, Axel; Thomas, Max; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6053 - 6059
• a: 9.8262 ± 0.0002 Å
• b: 15.8803 ± 0.0003 Å
• c: 23.2517 ± 0.0005 Å
• α: 102.676 ± 0.001°
• β: 101.007 ± 0.001°
• γ: 95.852 ± 0.001°
• Cell volume: 3435.29 ± 0.12 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0702
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.0806
• Weighted residual factors for all reflections included in the refinement: 0.0883
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No