Information card for entry 7039233

Structure parameters

• Formula: C84 H68 B Cl F24 N4 O8 Rh2
• Calculated formula: C84 H68 B Cl F24 N4 O8 Rh2
• Title of publication: Coordination chemistry of a calix[4]arene-based NHC ligand: dinuclear complexes and comparison to I(i)Pr2Me2.
• Authors of publication: Patchett, Ruth; Chaplin, Adrian B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 21
• Pages of publication: 8945 - 8955
• a: 19.6345 ± 0.0004 Å
• b: 22.6778 ± 0.0005 Å
• c: 20.0799 ± 0.0004 Å
• α: 90°
• β: 109.352 ± 0.003°
• γ: 90°
• Cell volume: 8435.8 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2973
• Residual factor for significantly intense reflections: 0.2744
• Weighted residual factors for significantly intense reflections: 0.6103
• Weighted residual factors for all reflections included in the refinement: 0.6304
• Goodness-of-fit parameter for all reflections included in the refinement: 2.559
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No