Information card for entry 7039234

Structure parameters

• Formula: C58 H52 B Cl F24 N4 O4 Rh2
• Calculated formula: C58 H52 B Cl F24 N4 O4 Rh2
• Title of publication: Coordination chemistry of a calix[4]arene-based NHC ligand: dinuclear complexes and comparison to I(i)Pr2Me2.
• Authors of publication: Patchett, Ruth; Chaplin, Adrian B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 21
• Pages of publication: 8945 - 8955
• a: 12.2319 ± 0.0003 Å
• b: 13.2693 ± 0.0003 Å
• c: 21.7143 ± 0.0004 Å
• α: 100.987 ± 0.0015°
• β: 94.9257 ± 0.0017°
• γ: 91.7507 ± 0.0018°
• Cell volume: 3443.07 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0566
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.107
• Weighted residual factors for all reflections included in the refinement: 0.1152
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No