Information card for entry 7041774

Structure parameters

• Formula: C28 H38 F7 K O6 Si3
• Calculated formula: C28 H38 F7 K O6 Si3
• Title of publication: Fluoride complexation by bidentate silicon Lewis acids.
• Authors of publication: Horstmann, Jan; Niemann, Mark; Berthold, Katarína; Mix, Andreas; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 6
• Pages of publication: 1898 - 1913
• a: 9.6707 ± 0.0003 Å
• b: 14.7072 ± 0.0003 Å
• c: 12.2271 ± 0.0003 Å
• α: 90°
• β: 100.137 ± 0.003°
• γ: 90°
• Cell volume: 1711.9 ± 0.08 ų
• Cell temperature: 99.93 ± 0.16 K
• Ambient diffraction temperature: 99.93 ± 0.16 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.1072
• Weighted residual factors for all reflections included in the refinement: 0.1116
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No