Information card for entry 7041773

Structure parameters

• Formula: C52 H90 F8 K2 N4 O12 Si3
• Calculated formula: C52 H90 F8 K2 N4 O12 Si3
• Title of publication: Fluoride complexation by bidentate silicon Lewis acids.
• Authors of publication: Horstmann, Jan; Niemann, Mark; Berthold, Katarína; Mix, Andreas; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 6
• Pages of publication: 1898 - 1913
• a: 11.42848 ± 0.00016 Å
• b: 14.5458 ± 0.0002 Å
• c: 20.6353 ± 0.0003 Å
• α: 101.002 ± 0.0012°
• β: 99.0164 ± 0.0012°
• γ: 106.203 ± 0.0012°
• Cell volume: 3152.29 ± 0.08 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0813
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No