Information card for entry 7041852

Structure parameters

• Formula: C90 H170 N2 O24 Si14 U
• Calculated formula: C90 H170 N2 O24 Si14 U
• Title of publication: Synthesis and structural study of new metallasilsesquioxanes of potassium and uranium.
• Authors of publication: Gießmann, Stephan; Lorenz, Volker; Liebing, Phil; Hilfert, Liane; Fischer, Axel; Edelmann, Frank T.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 8
• Pages of publication: 2415 - 2419
• a: 25.601 ± 0.001 Å
• b: 15.0671 ± 0.001 Å
• c: 30.8351 ± 0.001 Å
• α: 90°
• β: 102.059 ± 0.003°
• γ: 90°
• Cell volume: 11631.6 ± 1 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0707
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.0747
• Weighted residual factors for all reflections included in the refinement: 0.0851
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No