Information card for entry 7041923

Structure parameters

• Formula: C111 H87 Cl9 P6 Sb2
• Calculated formula: C111 H87 Cl9 P6 Sb2
• Title of publication: On the coordination non-innocence of antimony in nickel(ii) complexes of the tetradentate (o-(Ph2P)C6H4)3Sb ligand.
• Authors of publication: Jones, J. Stuart; Wade, Casey R.; Yang, Mengxi; Gabbaï, François P
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5598 - 5604
• a: 15.442 ± 0.005 Å
• b: 15.443 ± 0.005 Å
• c: 22.924 ± 0.008 Å
• α: 89.098 ± 0.018°
• β: 87.977 ± 0.018°
• γ: 60.383 ± 0.014°
• Cell volume: 4749 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0839
• Residual factor for significantly intense reflections: 0.0713
• Weighted residual factors for significantly intense reflections: 0.2193
• Weighted residual factors for all reflections included in the refinement: 0.2377
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No