Information card for entry 7041924

Structure parameters

• Formula: C159 H130 B2 Cl8 Ni2 P6 Sb2
• Calculated formula: C159 H130 B2 Cl8 Ni2 P6 Sb2
• Title of publication: On the coordination non-innocence of antimony in nickel(ii) complexes of the tetradentate (o-(Ph2P)C6H4)3Sb ligand.
• Authors of publication: Jones, J. Stuart; Wade, Casey R.; Yang, Mengxi; Gabbaï, François P
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5598 - 5604
• a: 49.945 ± 0.004 Å
• b: 9.67 ± 0.0009 Å
• c: 34.967 ± 0.003 Å
• α: 90°
• β: 129.231 ± 0.004°
• γ: 90°
• Cell volume: 13081 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0848
• Residual factor for significantly intense reflections: 0.062
• Weighted residual factors for significantly intense reflections: 0.1266
• Weighted residual factors for all reflections included in the refinement: 0.1353
• Goodness-of-fit parameter for all reflections included in the refinement: 1.158
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No