Information card for entry 7042868

Structure parameters

• Formula: C39 H47 Cl3 Fe Ge N2 O Si
• Calculated formula: C39 H47 Cl3 Fe Ge N2 O Si
• Title of publication: C4-Ferrocenylsilyl-bridged and -substituted N-heterocyclic carbenes: complexation of germanium chloride.
• Authors of publication: Wang, Yuzhong; Hickox, Hunter P.; Wei, Pingrong; Robinson, Gregory H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5508 - 5512
• a: 10.5862 ± 0.0005 Å
• b: 10.6734 ± 0.0005 Å
• c: 18.5264 ± 0.001 Å
• α: 85.038 ± 0.002°
• β: 84.783 ± 0.002°
• γ: 74.549 ± 0.002°
• Cell volume: 2005.07 ± 0.17 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1034
• Residual factor for significantly intense reflections: 0.0707
• Weighted residual factors for significantly intense reflections: 0.1598
• Weighted residual factors for all reflections included in the refinement: 0.177
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No