Information card for entry 7042869

Structure parameters

• Formula: C76 H106 Cl4 Fe Ge2 N4 O2 Si2
• Calculated formula: C76 H106 Cl4 Fe Ge2 N4 O2 Si2
• Title of publication: C4-Ferrocenylsilyl-bridged and -substituted N-heterocyclic carbenes: complexation of germanium chloride.
• Authors of publication: Wang, Yuzhong; Hickox, Hunter P.; Wei, Pingrong; Robinson, Gregory H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5508 - 5512
• a: 12.1909 ± 0.0009 Å
• b: 16.9634 ± 0.0012 Å
• c: 20.152 ± 0.0014 Å
• α: 80.614 ± 0.002°
• β: 82.073 ± 0.002°
• γ: 82.496 ± 0.002°
• Cell volume: 4047.3 ± 0.5 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1155
• Residual factor for significantly intense reflections: 0.0653
• Weighted residual factors for significantly intense reflections: 0.1599
• Weighted residual factors for all reflections included in the refinement: 0.1898
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No