Information card for entry 7042871

Structure parameters

• Formula: C33 H49 Cl N2 O Si
• Calculated formula: C33 H49 Cl N2 O Si
• Title of publication: C4-Ferrocenylsilyl-bridged and -substituted N-heterocyclic carbenes: complexation of germanium chloride.
• Authors of publication: Wang, Yuzhong; Hickox, Hunter P.; Wei, Pingrong; Robinson, Gregory H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5508 - 5512
• a: 8.935 ± 0.003 Å
• b: 12.508 ± 0.004 Å
• c: 16.628 ± 0.005 Å
• α: 69.021 ± 0.01°
• β: 81.901 ± 0.011°
• γ: 81.762 ± 0.011°
• Cell volume: 1709.2 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1017
• Residual factor for significantly intense reflections: 0.0636
• Weighted residual factors for significantly intense reflections: 0.1594
• Weighted residual factors for all reflections included in the refinement: 0.1803
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No