Information card for entry 7042872

Structure parameters

• Formula: C37 H43 Cl Fe N2 Si
• Calculated formula: C37 H43 Cl Fe N2 Si
• Title of publication: C4-Ferrocenylsilyl-bridged and -substituted N-heterocyclic carbenes: complexation of germanium chloride.
• Authors of publication: Wang, Yuzhong; Hickox, Hunter P.; Wei, Pingrong; Robinson, Gregory H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5508 - 5512
• a: 18.7276 ± 0.0013 Å
• b: 18.1214 ± 0.0012 Å
• c: 21.7095 ± 0.0015 Å
• α: 90°
• β: 112.148 ± 0.002°
• γ: 90°
• Cell volume: 6823.9 ± 0.8 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1661
• Residual factor for significantly intense reflections: 0.0766
• Weighted residual factors for significantly intense reflections: 0.1372
• Weighted residual factors for all reflections included in the refinement: 0.1667
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No