Information card for entry 7043072

Structure parameters

• Formula: C34.5 H59 Fe Ge N O Si3
• Calculated formula: C34.5 H59 Fe Ge1.005 N O Si3
• Title of publication: An Iron Germylene Complex Having Fe-H and Ge-H Bonds: Synthesis, Structure and Reactivity
• Authors of publication: Dhungana, Tara Prasad; Hashimoto, Hisako; Tobita, Hiromi
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 32.8319 ± 0.0014 Å
• b: 12.2428 ± 0.0005 Å
• c: 20.4141 ± 0.0009 Å
• α: 90°
• β: 109.345 ± 0.002°
• γ: 90°
• Cell volume: 7742.3 ± 0.6 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1019
• Residual factor for significantly intense reflections: 0.0753
• Weighted residual factors for significantly intense reflections: 0.1393
• Weighted residual factors for all reflections included in the refinement: 0.1484
• Goodness-of-fit parameter for all reflections included in the refinement: 1.185
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No