Information card for entry 7043073

Structure parameters

• Formula: C35 H57 Fe Ge N O2 Si3
• Calculated formula: C35 H57 Fe Ge N O2 Si3
• Title of publication: An Iron Germylene Complex Having Fe-H and Ge-H Bonds: Synthesis, Structure and Reactivity
• Authors of publication: Dhungana, Tara Prasad; Hashimoto, Hisako; Tobita, Hiromi
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 8.6833 ± 0.0007 Å
• b: 12.771 ± 0.001 Å
• c: 17.5545 ± 0.0009 Å
• α: 77.427 ± 0.002°
• β: 86.298 ± 0.003°
• γ: 80.826 ± 0.002°
• Cell volume: 1874.8 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0487
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.0933
• Weighted residual factors for all reflections included in the refinement: 0.097
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No