Crystallography Open Database

Information card for entry 7043401

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Coordinates	7043401.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H66 Li N5 Si2
Calculated formula	C44 H66 Li N5 Si2
Title of publication	Coordination Behavior of Bidentate Bis(carbenes) at Alkali Metal Bis(trimethylsilyl)amides
Authors of publication	Westerhausen, Matthias; Koch, Alexander; Görls, Helmar; Krieck, Sven
Journal of publication	Dalton Trans.
Year of publication	2017
a	11.9364 ± 0.0002 Å
b	23.8335 ± 0.0004 Å
c	15.9497 ± 0.0002 Å
α	90°
β	92.007 ± 0.001°
γ	90°
Cell volume	4534.69 ± 0.12 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0859
Residual factor for significantly intense reflections	0.0677
Weighted residual factors for significantly intense reflections	0.1662
Weighted residual factors for all reflections included in the refinement	0.1808
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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