Crystallography Open Database

Information card for entry 7043402

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Coordinates	7043402.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C88 H132 K2 N10 Si4
Calculated formula	C88 H132 K2 N10 Si4
Title of publication	Coordination Behavior of Bidentate Bis(carbenes) at Alkali Metal Bis(trimethylsilyl)amides
Authors of publication	Westerhausen, Matthias; Koch, Alexander; Görls, Helmar; Krieck, Sven
Journal of publication	Dalton Trans.
Year of publication	2017
a	11.8026 ± 0.0002 Å
b	12.4884 ± 0.0003 Å
c	16.4591 ± 0.0002 Å
α	92.514 ± 0.001°
β	103.129 ± 0.001°
γ	100.373 ± 0.001°
Cell volume	2314.86 ± 0.07 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0602
Residual factor for significantly intense reflections	0.0529
Weighted residual factors for significantly intense reflections	0.1161
Weighted residual factors for all reflections included in the refinement	0.1206
Goodness-of-fit parameter for all reflections included in the refinement	1.129
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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