Information card for entry 7045502

Structure parameters

• Formula: C15 H39 K N4 O Si3 Ti
• Calculated formula: C15 H39 K N4 O Si3 Ti
• Title of publication: Formate complexes of titanium(iv) supported by a triamido-amine ligand.
• Authors of publication: Paparo, A.; van Krüchten, F D; Spaniol, T. P.; Okuda, J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 10
• Pages of publication: 3530 - 3537
• a: 10.284 ± 0.0015 Å
• b: 10.5727 ± 0.0015 Å
• c: 23.865 ± 0.003 Å
• α: 90°
• β: 100.149 ± 0.003°
• γ: 90°
• Cell volume: 2554.2 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.0405
• Weighted residual factors for significantly intense reflections: 0.0882
• Weighted residual factors for all reflections included in the refinement: 0.0972
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No