Information card for entry 7045503

Structure parameters

• Formula: C44 H56 B Cl8 N5 Si3 Ti
• Calculated formula: C44 H56 B Cl8 N5 Si3 Ti
• Title of publication: Formate complexes of titanium(iv) supported by a triamido-amine ligand.
• Authors of publication: Paparo, A.; van Krüchten, F D; Spaniol, T. P.; Okuda, J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 10
• Pages of publication: 3530 - 3537
• a: 16.8069 ± 0.0018 Å
• b: 17.8453 ± 0.0019 Å
• c: 17.9679 ± 0.0019 Å
• α: 94.24 ± 0.002°
• β: 92.638 ± 0.003°
• γ: 92.916 ± 0.003°
• Cell volume: 5360.6 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1107
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.1271
• Weighted residual factors for all reflections included in the refinement: 0.1494
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No