Information card for entry 7045916

Structure parameters

• Formula: C32 H60 Ge Si8
• Calculated formula: C32 H60 Ge Si8
• Title of publication: Spirocyclic germanes via transannular insertion reactions of vinyl germylenes into Si-Si bonds.
• Authors of publication: Walewska, Małgorzata; Baumgartner, Judith; Marschner, Christoph; Albers, Lena; Müller, Thomas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 17
• Pages of publication: 5985 - 5996
• a: 9.7118 ± 0.0019 Å
• b: 27.874 ± 0.006 Å
• c: 16.028 ± 0.003 Å
• α: 90°
• β: 98.49 ± 0.03°
• γ: 90°
• Cell volume: 4291.3 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0933
• Residual factor for significantly intense reflections: 0.0871
• Weighted residual factors for significantly intense reflections: 0.1525
• Weighted residual factors for all reflections included in the refinement: 0.1548
• Goodness-of-fit parameter for all reflections included in the refinement: 1.394
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No