Information card for entry 7045917

Structure parameters

• Formula: C30 H58 Ge3 Si6
• Calculated formula: C30 H58 Ge3 Si6
• Title of publication: Spirocyclic germanes via transannular insertion reactions of vinyl germylenes into Si-Si bonds.
• Authors of publication: Walewska, Małgorzata; Baumgartner, Judith; Marschner, Christoph; Albers, Lena; Müller, Thomas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 17
• Pages of publication: 5985 - 5996
• a: 10.817 ± 0.003 Å
• b: 35.902 ± 0.009 Å
• c: 10.823 ± 0.003 Å
• α: 90°
• β: 96.083 ± 0.005°
• γ: 90°
• Cell volume: 4179.5 ± 1.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1116
• Residual factor for significantly intense reflections: 0.0894
• Weighted residual factors for significantly intense reflections: 0.1831
• Weighted residual factors for all reflections included in the refinement: 0.1923
• Goodness-of-fit parameter for all reflections included in the refinement: 1.182
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No