Information card for entry 7046264

Structure parameters

• Formula: C57 H46 B F4 N3 Ni3 O4.5 P3
• Calculated formula: C57 H46 B F4 N3 Ni3 O4.5 P3
• Title of publication: Ni(ii) complexes of the phosphine-oxime Ph₂PC₆H₄-2-CH[double bond, length as m-dash]NOH.
• Authors of publication: Basu, Debashis; Woods, Toby J.; Rauchfuss, Thomas B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 21
• Pages of publication: 7256 - 7262
• a: 14.4858 ± 0.0013 Å
• b: 14.8932 ± 0.0013 Å
• c: 15.1803 ± 0.0012 Å
• α: 91.309 ± 0.003°
• β: 108.166 ± 0.003°
• γ: 118.187 ± 0.003°
• Cell volume: 2685.6 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0719
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1021
• Weighted residual factors for all reflections included in the refinement: 0.108
• Goodness-of-fit parameter for all reflections included in the refinement: 1.134
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No