Information card for entry 7046265

Structure parameters

• Formula: C52.96 H36.64 Cl2.27 F10 N2 Ni2 O2 P2
• Calculated formula: C52.956 H36.64 Cl2.272 F10 N2 Ni2 O2 P2
• Title of publication: Ni(ii) complexes of the phosphine-oxime Ph₂PC₆H₄-2-CH[double bond, length as m-dash]NOH.
• Authors of publication: Basu, Debashis; Woods, Toby J.; Rauchfuss, Thomas B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 21
• Pages of publication: 7256 - 7262
• a: 11.3092 ± 0.0004 Å
• b: 14.2034 ± 0.0005 Å
• c: 16.4001 ± 0.0006 Å
• α: 90.312 ± 0.001°
• β: 100.835 ± 0.001°
• γ: 108.031 ± 0.001°
• Cell volume: 2454.58 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0733
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No