Information card for entry 7046917

Structure parameters

• Formula: C56 H124 Ce K O18 Si4
• Calculated formula: C56 H124 Ce K O18 Si4
• Title of publication: Redox-enhanced hemilability of a tris(tert-butoxy)siloxy ligand at cerium.
• Authors of publication: Friedrich, Jochen; Qiao, Yusen; Maichle-Mössmer, Cäcilia; Schelter, Eric J.; Anwander, Reiner
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 30
• Pages of publication: 10113 - 10123
• a: 22.496 ± 0.0009 Å
• b: 14.8753 ± 0.0004 Å
• c: 23.0312 ± 0.0007 Å
• α: 90°
• β: 106.034 ± 0.002°
• γ: 90°
• Cell volume: 7407.2 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0412
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0557
• Weighted residual factors for all reflections included in the refinement: 0.0599
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No