Information card for entry 7047271

Structure parameters

• Formula: C22 H39 N2 O2 P
• Calculated formula: C22 H39 N2 O2 P
• Title of publication: Lewis and Brønsted basicity of phosphine-diazomethane derivatives.
• Authors of publication: Schneider, Carolin; LaFortune, James H. W.; Melen, Rebecca L.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 36
• Pages of publication: 12742 - 12749
• a: 7.7213 ± 0.0008 Å
• b: 16.7703 ± 0.0018 Å
• c: 9.1967 ± 0.001 Å
• α: 90°
• β: 110.326 ± 0.004°
• γ: 90°
• Cell volume: 1116.7 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0596
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.0929
• Weighted residual factors for all reflections included in the refinement: 0.1093
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No