Information card for entry 7047272

Structure parameters

• Formula: C34 H35 B F15 N2 O3 P
• Calculated formula: C34 H35 B F15 N2 O3 P
• Title of publication: Lewis and Brønsted basicity of phosphine-diazomethane derivatives.
• Authors of publication: Schneider, Carolin; LaFortune, James H. W.; Melen, Rebecca L.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 36
• Pages of publication: 12742 - 12749
• a: 11.9153 ± 0.0011 Å
• b: 13.8962 ± 0.0011 Å
• c: 22.195 ± 0.002 Å
• α: 90°
• β: 93.783 ± 0.004°
• γ: 90°
• Cell volume: 3667 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0999
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for significantly intense reflections: 0.1217
• Weighted residual factors for all reflections included in the refinement: 0.1682
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No