Information card for entry 7047758

Structure parameters

• Formula: C75.31 H99.64 N18 O Si Yb
• Calculated formula: C59 H80 N18 O Si Yb
• Title of publication: Variable coordination of carbazolyl-bis(tetrazole) ligands in lanthanide chemistry.
• Authors of publication: Gajecki, Leah; Berg, David J.; Hoenisch, Josh; Oliver, Allen G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 43
• Pages of publication: 15487 - 15496
• a: 13.0237 ± 0.0013 Å
• b: 15.8464 ± 0.0015 Å
• c: 18.8408 ± 0.0019 Å
• α: 82.905 ± 0.003°
• β: 88.389 ± 0.003°
• γ: 87.902 ± 0.003°
• Cell volume: 3854.9 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.1263
• Weighted residual factors for all reflections included in the refinement: 0.1417
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.7749 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No