Information card for entry 7047759

Structure parameters

• Common name: [Sm(CzTiPr)2]2(mu-OH)2
• Chemical name: Sm(κ3-CzTiPr)(κ3-μ-CzTiPr)(μ-OH)2Sm(κ3-CzTiPr)(κ2-CzTiPr)
• Formula: C115.5 H148 N36 O2 Sm2
• Calculated formula: C115.5 H148 N36 O2 Sm2
• Title of publication: Variable coordination of carbazolyl-bis(tetrazole) ligands in lanthanide chemistry.
• Authors of publication: Gajecki, Leah; Berg, David J.; Hoenisch, Josh; Oliver, Allen G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 43
• Pages of publication: 15487 - 15496
• a: 16.49 ± 0.0019 Å
• b: 19.382 ± 0.002 Å
• c: 21.328 ± 0.002 Å
• α: 73.382 ± 0.003°
• β: 72.642 ± 0.003°
• γ: 89.771 ± 0.003°
• Cell volume: 6209.7 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1436
• Residual factor for significantly intense reflections: 0.0932
• Weighted residual factors for significantly intense reflections: 0.2425
• Weighted residual factors for all reflections included in the refinement: 0.2805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 1.0332 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No