Information card for entry 7047775

Structure parameters

• Common name: Hexa-zinc-18-tungstoantimonate
• Formula: C68 H109 N22 O94 Sb2 W18 Zn6
• Calculated formula: C68 H105 N22 O94.6 Sb2 W17.9 Zn6
• Title of publication: Synthesis of the first Zn₆-hexagon sandwich-tungstoantimonate via rearrangement of a non-lacunary Krebs-type polyoxotungstate.
• Authors of publication: Tanuhadi, Elias; Roller, Alexander; Giester, Gerald; Kampatsikas, Ioannis; Rompel, Annette
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 44
• Pages of publication: 15651 - 15655
• a: 12.4792 ± 0.0008 Å
• b: 17.4813 ± 0.0013 Å
• c: 17.6938 ± 0.0011 Å
• α: 94.425 ± 0.004°
• β: 109.14 ± 0.003°
• γ: 104.946 ± 0.004°
• Cell volume: 3467.5 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0683
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.1007
• Weighted residual factors for all reflections included in the refinement: 0.1124
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No