Information card for entry 7047776

Structure parameters

• Common name: (TMA)4Hexa-zinc-18-tungstoantimonate
• Formula: C16 H48 N4 O72 Sb2 W18 Zn6
• Calculated formula: C16 H48 N4 O72 Sb2 W18 Zn6
• Title of publication: Synthesis of the first Zn₆-hexagon sandwich-tungstoantimonate via rearrangement of a non-lacunary Krebs-type polyoxotungstate.
• Authors of publication: Tanuhadi, Elias; Roller, Alexander; Giester, Gerald; Kampatsikas, Ioannis; Rompel, Annette
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 44
• Pages of publication: 15651 - 15655
• a: 14.5029 ± 0.0012 Å
• b: 23.1699 ± 0.0012 Å
• c: 18.1162 ± 0.0011 Å
• α: 90°
• β: 95.44 ± 0.004°
• γ: 90°
• Cell volume: 6060.2 ± 0.7 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0783
• Residual factor for significantly intense reflections: 0.0753
• Weighted residual factors for significantly intense reflections: 0.1982
• Weighted residual factors for all reflections included in the refinement: 0.2026
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No