Information card for entry 7048002

Structure parameters

• Formula: C31 H49 N2 Ni O P
• Calculated formula: C31 H49 N2 Ni O P
• Title of publication: A comparative analysis of hydrosilative amide reduction catalyzed by first-row transition metal (Mn, Fe, Co, and Ni) N-phosphinoamidinate complexes.
• Authors of publication: Macaulay, Casper M.; Ogawa, Takahiko; McDonald, Robert; Sydora, Orson L.; Stradiotto, Mark; Turculet, Laura
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 26
• Pages of publication: 9581 - 9587
• a: 10.4874 ± 0.0004 Å
• b: 10.8569 ± 0.0004 Å
• c: 14.6279 ± 0.0005 Å
• α: 70.005 ± 0.0004°
• β: 85.1598 ± 0.0005°
• γ: 87.5815 ± 0.0005°
• Cell volume: 1559.41 ± 0.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.087
• Weighted residual factors for all reflections included in the refinement: 0.0897
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No