Information card for entry 7048003

Structure parameters

• Formula: C35 H49 N2 Ni O P
• Calculated formula: C35 H49 N2 Ni O P
• Title of publication: A comparative analysis of hydrosilative amide reduction catalyzed by first-row transition metal (Mn, Fe, Co, and Ni) N-phosphinoamidinate complexes.
• Authors of publication: Macaulay, Casper M.; Ogawa, Takahiko; McDonald, Robert; Sydora, Orson L.; Stradiotto, Mark; Turculet, Laura
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 26
• Pages of publication: 9581 - 9587
• a: 8.6286 ± 0.0003 Å
• b: 11.7724 ± 0.0004 Å
• c: 17.2358 ± 0.0006 Å
• α: 86.1898 ± 0.0004°
• β: 79.796 ± 0.0004°
• γ: 72.2523 ± 0.0004°
• Cell volume: 1640.96 ± 0.1 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0395
• Residual factor for significantly intense reflections: 0.0345
• Weighted residual factors for significantly intense reflections: 0.0908
• Weighted residual factors for all reflections included in the refinement: 0.0944
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No