Information card for entry 7048015

Structure parameters

• Formula: C70 H67 Cl F24 N15 O24 S8 Sn2
• Calculated formula: C70 H70 Cl F24 N15 O24 S8 Sn2
• Title of publication: Synthesis, characterization and mass-spectrometric analysis of [LSn(IV)F_4-x]^x+ salts [L = tris ((1-ethyl-benzoimidazol-2-yl)methyl)amine, x = 1-4].
• Authors of publication: Suter, Riccardo; Swidan, Ala'aeddeen; Zijlstra, Harmen S.; Macdonald, Charles L. B.; McIndoe, J. Scott; Burford, Neil
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 46
• Pages of publication: 16729 - 16736
• a: 13.3317 ± 0.0012 Å
• b: 17.1334 ± 0.0015 Å
• c: 42.567 ± 0.004 Å
• α: 90°
• β: 96.119 ± 0.002°
• γ: 90°
• Cell volume: 9667.6 ± 1.5 ų
• Cell temperature: 170 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0923
• Weighted residual factors for significantly intense reflections: 0.1945
• Weighted residual factors for all reflections included in the refinement: 0.198
• Goodness-of-fit parameter for all reflections included in the refinement: 1.288
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No