Information card for entry 7048016

Structure parameters

• Formula: C39 H48 F10 N7 O10 P S3 Sn
• Calculated formula: C39 H48 F10 N7 O10 P S3 Sn
• Title of publication: Synthesis, characterization and mass-spectrometric analysis of [LSn(IV)F_4-x]^x+ salts [L = tris ((1-ethyl-benzoimidazol-2-yl)methyl)amine, x = 1-4].
• Authors of publication: Suter, Riccardo; Swidan, Ala'aeddeen; Zijlstra, Harmen S.; Macdonald, Charles L. B.; McIndoe, J. Scott; Burford, Neil
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 46
• Pages of publication: 16729 - 16736
• a: 12.9482 ± 0.001 Å
• b: 13.7454 ± 0.001 Å
• c: 17.427 ± 0.0013 Å
• α: 81.027 ± 0.003°
• β: 71.795 ± 0.002°
• γ: 62.15 ± 0.002°
• Cell volume: 2604.9 ± 0.3 ų
• Cell temperature: 170 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for significantly intense reflections: 0.1131
• Weighted residual factors for all reflections included in the refinement: 0.1229
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No