Information card for entry 7048019

Structure parameters

• Formula: C39 H45 F6 N11 O3 S Sn
• Calculated formula: C39 H45 F6 N11 O3 S Sn
• Title of publication: Synthesis, characterization and mass-spectrometric analysis of [LSn(IV)F_4-x]^x+ salts [L = tris ((1-ethyl-benzoimidazol-2-yl)methyl)amine, x = 1-4].
• Authors of publication: Suter, Riccardo; Swidan, Ala'aeddeen; Zijlstra, Harmen S.; Macdonald, Charles L. B.; McIndoe, J. Scott; Burford, Neil
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 46
• Pages of publication: 16729 - 16736
• a: 24.1425 ± 0.0011 Å
• b: 14.5319 ± 0.0007 Å
• c: 24.5279 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8605.3 ± 0.7 ų
• Cell temperature: 170 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1028
• Residual factor for significantly intense reflections: 0.0602
• Weighted residual factors for significantly intense reflections: 0.1241
• Weighted residual factors for all reflections included in the refinement: 0.1648
• Goodness-of-fit parameter for all reflections included in the refinement: 1.239
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No