Synthesis, characterization and mass-spectrometric analysis of [LSn(IV)F<sub>4-x</sub>]<sup>x+</sup> salts [L = tris ((1-ethyl-benzoimidazol-2-yl)methyl)amine, x = 1-4].
Authors of publication
Suter, Riccardo; Swidan, Ala'aeddeen; Zijlstra, Harmen S.; Macdonald, Charles L. B.; McIndoe, J. Scott; Burford, Neil
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2018
Journal volume
47
Journal issue
46
Pages of publication
16729 - 16736
a
14.3989 ± 0.0011 Å
b
15.9087 ± 0.0013 Å
c
18.4727 ± 0.0014 Å
α
90°
β
92.894 ± 0.002°
γ
90°
Cell volume
4226.1 ± 0.6 Å3
Cell temperature
170 K
Ambient diffraction temperature
170 K
Number of distinct elements
7
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1098
Residual factor for significantly intense reflections
0.0692
Weighted residual factors for significantly intense reflections
0.1308
Weighted residual factors for all reflections included in the refinement
0.1768
Goodness-of-fit parameter for all reflections included in the refinement
