Information card for entry 7048646

Structure parameters

• Formula: C19 H19 N2 P
• Calculated formula: C19 H19 N2 P
• Title of publication: PNN' & P₂NN' ligands via reductive amination with phosphine aldehydes: synthesis and base-metal coordination chemistry.
• Authors of publication: Gradiski, Matthew V.; Tsui, Brian T. H.; Lough, Alan J.; Morris, Robert H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 6
• Pages of publication: 2150 - 2159
• a: 18.465 ± 0.0019 Å
• b: 5.4113 ± 0.0005 Å
• c: 17.7373 ± 0.0018 Å
• α: 90°
• β: 116.474 ± 0.003°
• γ: 90°
• Cell volume: 1586.5 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1133
• Weighted residual factors for all reflections included in the refinement: 0.1256
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No