Information card for entry 7048647

Structure parameters

• Formula: C34 H34 Cl2 Fe N2 P2
• Calculated formula: C34 H34 Cl2 Fe N2 P2
• Title of publication: PNN' & P₂NN' ligands via reductive amination with phosphine aldehydes: synthesis and base-metal coordination chemistry.
• Authors of publication: Gradiski, Matthew V.; Tsui, Brian T. H.; Lough, Alan J.; Morris, Robert H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 6
• Pages of publication: 2150 - 2159
• a: 7.578 ± 0.0008 Å
• b: 12.4245 ± 0.0014 Å
• c: 16.9432 ± 0.0019 Å
• α: 77.923 ± 0.004°
• β: 83.039 ± 0.003°
• γ: 81.784 ± 0.003°
• Cell volume: 1537 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1025
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.0709
• Weighted residual factors for all reflections included in the refinement: 0.085
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No