Information card for entry 7048648

Structure parameters

• Formula: C23 H21 Cl2 Co N2 P
• Calculated formula: C23 H21 Cl2 Co N2 P
• Title of publication: PNN' & P₂NN' ligands via reductive amination with phosphine aldehydes: synthesis and base-metal coordination chemistry.
• Authors of publication: Gradiski, Matthew V.; Tsui, Brian T. H.; Lough, Alan J.; Morris, Robert H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 6
• Pages of publication: 2150 - 2159
• a: 10.1359 ± 0.0008 Å
• b: 11.6672 ± 0.0011 Å
• c: 18.8632 ± 0.0016 Å
• α: 90°
• β: 96.513 ± 0.002°
• γ: 90°
• Cell volume: 2216.3 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1052
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0748
• Weighted residual factors for all reflections included in the refinement: 0.0938
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No