Information card for entry 7048776

Structure parameters

• Formula: C39 H36 N P Yb2
• Calculated formula: C39 H36 N P Yb2
• Title of publication: Generation and reactivity of neutral 1,3-benzazaphosphole and anionic 1,3-benzazaphospholide ytterbium(iii) complexes.
• Authors of publication: Ying, Huacheng; Gong, Mingzhu; Pi, Chengfu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 8
• Pages of publication: 2722 - 2729
• a: 38.22 ± 0.006 Å
• b: 8.3463 ± 0.0014 Å
• c: 22.987 ± 0.004 Å
• α: 90°
• β: 115.923 ± 0.003°
• γ: 90°
• Cell volume: 6594.9 ± 1.9 ų
• Cell temperature: 296.15 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0805
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1327
• Weighted residual factors for all reflections included in the refinement: 0.1445
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No