Information card for entry 7048777

Structure parameters

• Formula: C48 H27 B F15 N P Yb
• Calculated formula: C48 H27 B F15 N P Yb
• Title of publication: Generation and reactivity of neutral 1,3-benzazaphosphole and anionic 1,3-benzazaphospholide ytterbium(iii) complexes.
• Authors of publication: Ying, Huacheng; Gong, Mingzhu; Pi, Chengfu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 8
• Pages of publication: 2722 - 2729
• a: 13.2386 ± 0.0006 Å
• b: 21.6434 ± 0.001 Å
• c: 15.4959 ± 0.0007 Å
• α: 90°
• β: 102.1 ± 0.001°
• γ: 90°
• Cell volume: 4341.4 ± 0.3 ų
• Cell temperature: 100.15 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.036
• Residual factor for significantly intense reflections: 0.0264
• Weighted residual factors for significantly intense reflections: 0.0604
• Weighted residual factors for all reflections included in the refinement: 0.0645
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No