Information card for entry 7048826

Structure parameters

• Formula: C20 H31 N2 O Sb Si2
• Calculated formula: C20 H31 N2 O Sb Si2
• Title of publication: A study of di(amino)stibines with terminal Sb(iii) hydrogen-ligands by X-ray- and neutron-diffraction.
• Authors of publication: Schwamm, Ryan J.; Edwards, Alison J.; Fitchett, Christopher M.; Coles, Martyn P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 2953 - 2958
• a: 7.6028 ± 0.0005 Å
• b: 11.5896 ± 0.0008 Å
• c: 13.802 ± 0.0007 Å
• α: 99.459 ± 0.005°
• β: 100.012 ± 0.005°
• γ: 107.557 ± 0.006°
• Cell volume: 1110.98 ± 0.13 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1572
• Residual factor for significantly intense reflections: 0.0677
• Weighted residual factors for all reflections: 0.1429
• Weighted residual factors for significantly intense reflections: 0.0624
• Weighted residual factors for all reflections included in the refinement: 0.0537
• Goodness-of-fit parameter for all reflections included in the refinement: 1.4721
• Diffraction radiation probe: neutron
• Diffraction radiation wavelength: 0.85 Å
• Diffraction radiation type: neutron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No