Information card for entry 7048827

Structure parameters

• Formula: C62 H108 N4 O2 Sb2 Si4
• Calculated formula: C62 H108 N4 O2 Sb2 Si4
• Title of publication: A study of di(amino)stibines with terminal Sb(iii) hydrogen-ligands by X-ray- and neutron-diffraction.
• Authors of publication: Schwamm, Ryan J.; Edwards, Alison J.; Fitchett, Christopher M.; Coles, Martyn P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 2953 - 2958
• a: 12.3588 ± 0.0002 Å
• b: 16.881 ± 0.0004 Å
• c: 17.0204 ± 0.0004 Å
• α: 73.916 ± 0.002°
• β: 84.828 ± 0.0016°
• γ: 85.4219 ± 0.0016°
• Cell volume: 3392.47 ± 0.13 ų
• Cell temperature: 120.01 ± 0.1 K
• Ambient diffraction temperature: 120.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0382
• Residual factor for significantly intense reflections: 0.0302
• Weighted residual factors for significantly intense reflections: 0.0649
• Weighted residual factors for all reflections included in the refinement: 0.0685
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No