Information card for entry 7048828

Structure parameters

• Formula: C28 H46 Cl N2 O Sb Si2
• Calculated formula: C28 H46 Cl N2 O Sb Si2
• Title of publication: A study of di(amino)stibines with terminal Sb(iii) hydrogen-ligands by X-ray- and neutron-diffraction.
• Authors of publication: Schwamm, Ryan J.; Edwards, Alison J.; Fitchett, Christopher M.; Coles, Martyn P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 2953 - 2958
• a: 9.43069 ± 0.00012 Å
• b: 22.2904 ± 0.0003 Å
• c: 23.4692 ± 0.0003 Å
• α: 102.917 ± 0.001°
• β: 99.8049 ± 0.001°
• γ: 96.059 ± 0.001°
• Cell volume: 4685.18 ± 0.11 ų
• Cell temperature: 286.04 ± 0.1 K
• Ambient diffraction temperature: 286.04 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0692
• Weighted residual factors for all reflections included in the refinement: 0.0758
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No