Information card for entry 7048901

Structure parameters

• Formula: C118 H122 B2 F48 N2 P4 Rh2
• Calculated formula: C118 H122 B2 F48 N2 P4 Rh2
• Title of publication: A convenient method for the generation of {Rh(PNP)}⁺ and {Rh(PONOP)}⁺ fragments: reversible formation of vinylidene derivatives.
• Authors of publication: Gyton, Matthew R.; Hood, Thomas M.; Chaplin, Adrian B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 2877 - 2880
• a: 14.8856 ± 0.0003 Å
• b: 14.9585 ± 0.0003 Å
• c: 16.6238 ± 0.0003 Å
• α: 90.5493 ± 0.0016°
• β: 107.193 ± 0.0018°
• γ: 116.472 ± 0.002°
• Cell volume: 3121.85 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0408
• Residual factor for significantly intense reflections: 0.0355
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No