Information card for entry 7048905

Structure parameters

• Formula: C69 H73 B F24 N O2 P2 Rh
• Calculated formula: C69 H73 B F24 N O2 P2 Rh
• Title of publication: A convenient method for the generation of {Rh(PNP)}⁺ and {Rh(PONOP)}⁺ fragments: reversible formation of vinylidene derivatives.
• Authors of publication: Gyton, Matthew R.; Hood, Thomas M.; Chaplin, Adrian B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 2877 - 2880
• a: 12.52895 ± 0.00011 Å
• b: 16.71426 ± 0.00019 Å
• c: 20.3652 ± 0.0002 Å
• α: 66.149 ± 0.0011°
• β: 73.5696 ± 0.0009°
• γ: 80.0085 ± 0.0009°
• Cell volume: 3732.72 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0549
• Weighted residual factors for significantly intense reflections: 0.1484
• Weighted residual factors for all reflections included in the refinement: 0.1518
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No