Information card for entry 7049008

Structure parameters

• Formula: C26 H46 Ni P2 Si4
• Calculated formula: C26 H46 Ni P2 Si4
• Title of publication: Isolation of two bis(silyl)nickel complexes with Si-Si bond formation in a single-crystal-to-single-crystal fashion.
• Authors of publication: Zhang, Sen-Yu; Li, Jie; Zhao, Sheng-Ze; Wang, Shi; Lu, Min-Ming; Li, Yong-Hua; Huang, Wei
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 10
• Pages of publication: 3433 - 3439
• a: 12.4689 ± 0.0008 Å
• b: 12.4689 ± 0.0008 Å
• c: 20.552 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3195.3 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 116
• Hermann-Mauguin space group symbol: P -4 c 2
• Hall space group symbol: P -4 -2c
• Residual factor for all reflections: 0.0326
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.0535
• Weighted residual factors for all reflections included in the refinement: 0.0542
• Goodness-of-fit parameter for all reflections included in the refinement: 0.891
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No