Information card for entry 7049009

Structure parameters

• Formula: C32 H61 Ni P3 Si4
• Calculated formula: C32 H61 Ni P3 Si4
• Title of publication: Isolation of two bis(silyl)nickel complexes with Si-Si bond formation in a single-crystal-to-single-crystal fashion.
• Authors of publication: Zhang, Sen-Yu; Li, Jie; Zhao, Sheng-Ze; Wang, Shi; Lu, Min-Ming; Li, Yong-Hua; Huang, Wei
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 10
• Pages of publication: 3433 - 3439
• a: 11.352 ± 0.002 Å
• b: 21.355 ± 0.004 Å
• c: 15.654 ± 0.003 Å
• α: 90°
• β: 100.59 ± 0.03°
• γ: 90°
• Cell volume: 3730.2 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0556
• Residual factor for significantly intense reflections: 0.0444
• Weighted residual factors for significantly intense reflections: 0.1083
• Weighted residual factors for all reflections included in the refinement: 0.1118
• Goodness-of-fit parameter for all reflections included in the refinement: 0.955
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No