Information card for entry 7049038

Structure parameters

• Formula: C56 H59 B O4 Os P2
• Calculated formula: C56 H59 B O4 Os P2
• Title of publication: Pentamethylcyclopentadienyl osmium complexes that contain diazoalkane, dioxygen and allenylidene ligands: preparation and reactivity.
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; Sibilla, Francesca
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 3116 - 3131
• a: 17.0342 ± 0.0008 Å
• b: 16.7169 ± 0.0009 Å
• c: 18.298 ± 0.001 Å
• α: 90°
• β: 104.281 ± 0.002°
• γ: 90°
• Cell volume: 5049.5 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.026
• Weighted residual factors for significantly intense reflections: 0.0561
• Weighted residual factors for all reflections included in the refinement: 0.06
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No